1. 那位同志有XRD用的FeO、Fe3O4、CaO、Fe的pdf卡片啊,不用软件就能看的图片也行
我有JADY5,里面有较多的XRD卡片,但是一个物质晶形不同会有不同的XRD卡片Iron
Fe
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= d-Cutoff= I/Ic(RIR)=10.77
Ref= Level-1 PDF
Cubic, Im-3m(229) Z=2 mp=
Cell=2.867x2.867x2.867<90x90x90> Pearson=
Density(c)=7.869 Density(m)= Mwt= Vol=
Ref= Ibid.
Strong Line: 2.03/X 1.17/2 1.43/1 0.91/1
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
2.027 100.0 100.0 1 1 0 2 44.662 22.331 0.2466 3.0993
1.433 11.6 16.4 2 0 0 4 65.006 32.503 0.3488 4.3831
1.170 17.4 30.1 2 1 1 6 82.311 41.156 0.4272 5.3682
1.013 4.5 9.0 2 2 0 8 98.913 49.457 0.4933 6.1986
0.906 6.2 13.9 3 1 0 10 116.339 58.170 0.5515 6.9303
0.827 1.7 4.2 2 2 2 12 137.089 68.545 0.6041 7.5918
这样的结果你看得懂不?
2. XRD分析混合物,几种物质的PDF卡片峰位置和衍射图峰位置重叠,如何分析呀,请赐教!
按照衍射图位,单纯图位是可以重合的,可判断为包含;复合图位的,需要叠加后判断,叠加后重合为包含。
3. 跪求标准XRD的标准PDF卡片
Crystal system: Tetragonal
Space group: I4/mmm
Space group number: 139
a (?): 3.8618
b (?): 3.8618
c (?): 20.3544
Alpha (°): 90.0000
Beta (°): 90.0000
Gamma (°): 90.0000
No. h k l d [A] 2Theta[deg] I [%]
1 0 0 2 10.17720 8.682 3.9
2 0 0 4 5.08860 17.414 0.9
3 1 0 1 3.79413 23.428 9.9
4 0 0 6 3.39240 26.249 8.1
5 1 0 3 3.35623 26.537 3.6
6 1 0 5 2.80171 31.917 100.0
7 1 1 0 2.73072 32.770 65.4
8 1 1 2 2.63743 33.963 0.6
9 0 0 8 2.54430 35.246 1.1
10 1 1 4 2.40615 37.343 2.9
11 1 0 7 2.32292 38.733 7.0
12 1 1 6 2.12719 42.461 24.4
13 0 0 10 2.03544 44.475 13.0
14 1 0 9 1.95157 46.496 3.4
15 2 0 0 1.93091 47.023 34.8
16 2 0 2 1.89707 47.914 0.2
17 1 1 8 1.86151 48.888 1.9
18 2 0 4 1.80531 50.515 0.1
19 2 1 1 1.72087 53.182 2.0
20 0 0 12 1.69620 54.018 2.6
21 2 0 6 1.67812 54.648 3.8
22 2 1 3 1.67369 54.805 3.0
23 1 0 11 1.66873 54.982 5.4
24 1 1 10 1.63196 56.330 12.4
25 2 1 5 1.58990 57.959 29.3
26 2 0 8 1.53812 60.107 0.7
27 2 1 7 1.48489 62.498 2.6
28 0 0 14 1.45389 63.987 0.5
29 1 0 13 1.45100 64.129 0.3
30 1 1 12 1.44086 64.635 3.1
31 2 0 10 1.40086 66.717 11.3
32 2 1 9 1.37260 68.277 1.6
33 2 2 0 1.36536 68.690 8.4
34 2 2 2 1.35324 69.393 0.1
35 2 2 4 1.31871 71.483 0.1
36 3 0 1 1.28471 73.681 0.5
37 1 1 14 1.28333 73.774 0.8
38 1 0 15 1.28023 73.982 1.8
39 2 0 12 1.27434 74.381 3.2
40 0 0 16 1.27215 74.531 1.8
41 2 2 6 1.26662 74.912 1.5
42 2 1 11 1.26257 75.194 3.8
43 3 0 5 1.22737 77.747 5.2
44 3 1 0 1.22121 78.214 6.9
45 3 1 2 1.21252 78.883 0.1
46 2 2 8 1.20308 79.624 0.3
47 3 1 4 1.18750 80.883 0.3
48 3 0 7 1.17709 81.750 0.5
49 2 0 14 1.16146 83.091 0.8
50 1 1 16 1.15315 83.825 2.3
51 3 1 6 1.14903 84.195 4.2
52 1 0 17 1.14361 84.686 3.5
53 2 2 10 1.13388 85.586 4.5
54 0 0 18 1.13080 85.875 2.4
55 3 0 9 1.11874 87.030 0.3
56 3 1 8 1.10096 88.800 0.5
4. 请教XRD中的PDF卡片的含义
Pdf卡片是粉末衍射文件,每张卡片是一个纯物相的衍射峰数据,主要用来和我们的样品衍射结果进行比对,定性分析我们的样品里面有哪些物相!
5. 求pdf2004卡片库...
http://..com/link?url=99oA29UJQ8najA-wAoskSq39N4C--CxSaGEkRTpFa1JubXd6syf11gV-Pks3GKt9G-o_1mQWZS
6. Znic Zn 区别 请问谁知道XRD图谱中 PDF卡片中的Znic 何Zn 有什么区别
在XRD谱的PDF卡片中,第4区:晶体学参数区——
晶系(Sys.),空间群(S. G. ,前面是国际符号,后面是熊夫利符号),晶胞数据(a0,b0,c0),轴率(A= a0/b0,C= c0/b0),轴角α、β、γ。单位晶胞内分子数(Z),单位晶胞体积(V),Ref (该区数据参考文献)。
其中,Zn,代表单位晶胞内分子数是n。如CaTiO3,它的晶体结构是CaO·TiO2;PDF卡片中,写着Z64,代表单位晶胞内分子数是64。如果是高聚物,Z后面跟着的是单体单元数。不知是不是Znic。
你说的“Znic Zn ”要看出现在什么地方?上面说的Zn是出现在卡片中的“晶胞数据(a0,b0,c0),轴率(A= a0/b0,C= c0/b0),轴角α、β、γ。单位晶胞内分子数(Z),单位晶胞体积(V)”中。
如果是出现在介绍化合物的语句中,就有可能是把“Zinc”混为“Znic”(铝)。Zinc就是Zn,是铝的原子符号或缩写。用Google搜索“Znic Zn”,能够找到许多“Zinc”与“Znic”相混淆的词语的实例!
中国合格评定国家认可委员会- 机械,电子文档资料
GB/T5009.14-2003《 Determination of zinc in foods》 ...... GB8820-1988 《Food itives-Znic gluconate》 306 deoxidize matter ...... GB16355-1996 《Radiological protection standard for X-ray diffraction and fluorescence analysis equipment》 .... 球形喷口 · TF超耐力空压机油pdf · KL递进分配器 · 扩展新技术的梅特勒-托利多 ...
Mg掺杂ZnO纳米晶的低温共沉淀法制备及光学性质_网络文库
2010年12月6日 ... 1 图1 ( a) 纯ZnO, 掺杂ZnO 纳米晶的XRD 谱图; ( b) Mg Mg 石蜡, 纯氧化锌, .... Yellowishwhite luminescence in codoped znic oxide [ . ...
掺杂ZnO光学性质及染料敏化太阳能电池研究_网络文库
2010年12月10日... 兰州大学博上论文Abstract Znic oxide(ZnO),a ...
沉积电流对ZnO薄膜的结构和光学性质的影响Influence of Deposition ...
XRD分析表明ZnO薄膜为纤锌矿结构,晶粒尺寸随电流的增大而增大,择优取向随电流的变化发生了转变. ... 下载PDF阅读器. 摘要:: 采用阴极电沉积的方法在导电玻璃上制备了ZnO薄膜. ... films prepared by the oxidation of the metallic Zn [外文期刊] 1999(18) ... chemical-vapor deposition using znic acelacetonate and ozone [外文期刊] ...
[PDF] 150化学
文件格式: PDF/Adobe Acrobat - 快速查看
Znic(II) Complex Containing. Benzimidazolyl f刊,中】/朱 ...... characterization dinuclear of zn(II)一 ...... 采用XRD,BET,H2一TPR,TEM{41XPS ...
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文件格式: PDF/Adobe Acrobat
作者:ZQ Zhang - 2004 - 相关文章
合成硫化锌掺杂锰之萤光粉,借由不同之烧结温度,使用XRD及Raman ... Zinc sulfide ( ZnS ), as a II-VI semiconctor with a band gap energy of ...... 究,400 nm 的光是由锌空位(znic vacancies)所造成,425 nm 的光是由 ...
比较例句翻译_句库_爱词霸英语
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Find Sell Zinc powder, zn powder, Coatings Selling Leads offered by Qinhuang Taiji Ring Nano-Procts Co.,Ltd from China at TradeKey.com.
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7. jade5.0 ICDD pdf卡片库
去小木虫论坛找,很多很专业人士都在里面呢。
还有很多其他论坛,分析测试网络网,海川化工论坛等,应该去这样的论坛找啊。
8. 如何导出jade里的pdf卡片
导出jade里的pdf卡片的方法
可以导出的,步骤如下:
Flie-Print setup 然后你进入到一个可以打印的页面,
在上面可以添加标注的文字,
编辑完成后点击左上角第二个按钮即按钮,
选择 bitmap image ,
在word中点击粘贴就行了。
9. 请求高手帮忙分析XRD,自己不是很会学了一天,PDF卡片52-1140具体是什么
不好意思,一下子按错了。54-1140就当是免费赠送啦,细节就不说了,你按照下面的参照一下吧。
PDF#52-1140: QM=Star(+); d=Diffractometer; I=Diffractometer
Iron Silicon Oxide (铁氧化硅薄膜)
Fe2.95 Si0.05 O4
Radiation=CoKa1 Lambda=1.7896 Filter=
Calibration= d-Cutoff= I/Ic(RIR)=
Ref= Ohtaka, O., Tobe, H., Yamanaka, T.
Phys. Chem. Miner., 24 555 (1997)
Cubic - Powder Diffraction, F Z=8 mp=
Cell=8.388 Pearson=cF56 (Spinel, Al2 Mg O4)
Density(c)=5.181 Density(m)=5.10A Mwt=230.15 Vol=590.17 F(9)=82.7(.0099,11)
Ref= Ibid.
Strong Line: 2.53/X 1.61/4 2.10/3 1.48/3 2.97/3 1.71/1 4.84/1 2.42/1 1.92/1 0.00/1
NOTE: A mixture of Fe3 O4 and $GA-Fe2 Si O4 (molar ratio 9:1) was held for 5 hours at 1200 C and 6 GPa pressure.
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
4.844 6.0 3.0 1 1 1 3 18.300 9.150 0.1032 1.2971
2.966 26.0 22.0 2 2 0 8 30.105 15.052 0.1686 2.1184
2.529 100.0 100.0 3 1 1 11 35.466 17.733 0.1977 2.4845
2.421 3.0 3.0 2 2 2 12 37.104 18.552 0.2065 2.5953
2.096 33.0 40.0 4 0 0 16 43.123 21.562 0.2385 2.9977
1.924 1.0 1.0 3 3 1 19 47.201 23.600 0.2599 3.2657
1.712 7.0 10.0 4 2 2 24 53.478 26.739 0.2921 3.6701
1.614 38.0 60.0 5 1 1 27 57.012 28.506 0.3098 3.8929
1.483 32.0 55.0 4 4 0 32 62.585 31.292 0.3372 4.2368
PDF#54-1140: QM=Star(+); d=Diffractometer; I=Diffractometer (pdf#54-1140,采用测量衍射线相对强度方法:衍射仪法)
Aluminum Gadolinium Lanthanum Oxide(物质英文名,中文(有道词典翻译)名铝氧化钆镧系)
Gd0.68 La0.32 Al O3 (Yellowish) (物质化学式,含有Gd,La,Al,O元素,颜色淡黄)
Radiation=Sync Lambda=1.21893 Filter=Ge (检测用X射线,由同步发生,波长=1.21893nm,滤波片是Ge)
Calibration= d-Cutoff= I/Ic(RIR)= (校准,该物质最强线与刚玉最强线比值=)
Ref= Vasylechko, L., L'viv Polytechnic National Univ., Ukraine. (以上资料文献来源:Vasylechko, L., L'viv Polytechnic National Univ., Ukraine.)
ICDD Grant-in-Aid (2003) (国家衍射数据中心2003资助)
Orthorhombic - (Unknown), Pbnm (62) Z=4 mp= (正交晶系,一个单包中含有4个分子)
Cell=5.3068x5.3021x7.4908 Pearson=oP20 (?) (晶胞参数=x*y*z=5.3068x5.3021x7.4908 皮尔逊符号(描写晶体结构的):oP20)
Density(c)=7.115 Density(m)=5.97A Mwt=226.36 Vol=210.77 F(30)=19.7(0.029,52) (密度7.115 X射线密度5.97A 分子量226.36 晶胞体积210.77 )
Ref= Ibid. (参考文献,同上)
Strong Line: 2.65/X 3.74/5 1.87/3 1.53/3 2.16/3 1.32/3 1.68/2 1.00/2 1.19/2 1.18/1 (强峰)
NOTE: Single crystal was grown by the Czochralsky method (Louttz, G., Center for Material Research, Norfolk State Univ., Virginia, USA). (注:单晶由Czochralsky方法生长而成,作者Louttz,g。 材料研究中心,诺福克州立大学,美国维吉尼亚州)
Pattern taken at 25 C. (样品在25℃下制备)
Reference reports: a=5.3116(2), b=5.3061(2), c=7.4972(2). (参考报告:晶胞参数a,b,c)
Cell parameters generated by least squares refinement. (晶胞参数由最小二乘法得出)
(以下是XRD图的具体信息,可通过origin等软件做出XRD等图)
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
3.742 48.2 34.1 1 1 0 23.758 11.879 0.1336 1.6791
3.736 18.5 13.1 0 0 2 23.791 11.896 0.1338 1.6814
3.347 2.7 2.1 1 1 1 26.610 13.305 0.1494 1.8772
2.649 27.7 27.7 2 0 0 33.801 16.900 0.1887 2.3713
2.646 100.0 100.0 1 1 2 33.841 16.920 0.1889 2.3740
2.646 100.0 100.0 0 2 0 33.841 16.920 0.1889 2.3740
2.495 1.8 1.9 0 2 1 35.955 17.978 0.2003 2.5176
2.259 1.3 1.5 1 2 1 39.858 19.929 0.2213 2.7804
2.259 1.3 1.5 2 1 1 39.858 19.929 0.2213 2.7804
2.257 0.8 0.9 1 0 3 39.903 19.952 0.2215 2.7834
2.163 24.6 30.1 2 0 2 41.722 20.861 0.2311 2.9047
2.161 27.0 33.1 0 2 2 41.753 20.876 0.2313 2.9068
2.076 0.8 1.0 1 1 3 43.551 21.776 0.2408 3.0260
1.874 32.2 45.5 2 2 0 48.540 24.270 0.2668 3.3528
1.871 14.4 20.4 0 0 4 48.609 24.305 0.2672 3.3573
1.817 2.1 3.1 2 2 1 50.139 25.069 0.2750 3.4562
1.816 1.3 1.9 0 2 3 50.186 25.093 0.2753 3.4593
1.718 0.7 1.1 1 2 3 53.247 26.624 0.2909 3.6554
1.718 0.7 1.1 2 1 3 53.247 26.624 0.2909 3.6554
1.677 6.7 10.6 3 1 0 54.682 27.341 0.2981 3.7464
1.675 20.7 32.7 2 2 2 54.727 27.363 0.2984 3.7492
1.675 20.7 32.7 1 3 0 54.727 27.363 0.2984 3.7492
1.674 11.5 18.2 1 1 4 54.773 27.387 0.2986 3.7522
1.636 0.5 0.8 3 1 1 56.166 28.083 0.3056 3.8399
1.635 3.3 5.3 1 3 1 56.203 28.102 0.3058 3.8422
1.530 24.1 41.7 3 1 2 60.427 30.214 0.3267 4.1048
1.529 31.8 55.1 1 3 2 60.477 30.238 0.3269 4.1079
1.529 31.8 55.1 2 0 4 60.477 30.238 0.3269 4.1079
1.528 10.6 18.3 0 2 4 60.507 30.253 0.3270 4.1097
1.498 0.8 1.4 2 2 3 61.846 30.923 0.3336 4.1918
1.442 0.3 0.6 3 0 3 64.532 32.266 0.3465 4.3546
1.442 0.3 0.6 3 2 1 64.532 32.266 0.3465 4.3546
1.441 0.2 0.4 1 0 5 64.611 32.305 0.3469 4.3594
1.391 2.6 4.9 3 1 3 67.218 33.609 0.3593 4.5151
1.391 2.6 4.9 1 3 3 67.218 33.609 0.3593 4.5151
1.326 4.2 8.4 4 0 0 71.001 35.500 0.3769 4.7368
1.324 26.2 52.4 2 2 4 71.099 35.549 0.3774 4.7425
1.324 26.2 52.4 0 4 0 71.099 35.549 0.3774 4.7425
1.304 1.7 3.4 0 4 1 72.356 36.178 0.3832 4.8151
1.304 0.1 0.2 0 2 5 72.414 36.207 0.3834 4.8184
1.285 0.1 0.2 1 4 0 73.603 36.802 0.3889 4.8864
1.268 0.5 1.0 4 1 1 74.792 37.396 0.3942 4.9539
1.267 0.4 0.8 2 3 3 74.883 37.441 0.3946 4.9591
1.267 0.4 0.8 1 4 1 74.883 37.441 0.3946 4.9591
1.250 3.9 8.3 3 3 0 76.059 38.029 0.3999 5.0253
1.250 3.9 8.3 4 0 2 76.059 38.029 0.3999 5.0253
1.249 8.6 18.2 0 4 2 76.113 38.057 0.4001 5.0283
1.249 8.6 18.2 3 1 4 76.113 38.057 0.4001 5.0283
1.249 8.4 17.8 1 3 4 76.154 38.077 0.4003 5.0306
1.248 1.1 2.3 0 0 6 76.212 38.106 0.4006 5.0338
1.233 1.4 3.0 3 3 1 77.316 38.658 0.4055 5.0954
1.186 5.7 12.7 4 2 0 80.975 40.487 0.4215 5.2962
1.185 16.1 35.9 2 4 0 81.031 40.515 0.4217 5.2992
1.185 16.1 35.9 3 3 2 81.031 40.515 0.4217 5.2992
1.184 12.0 26.8 1 1 6 81.132 40.566 0.4221 5.3047
1.171 0.6 1.4 4 2 1 82.204 41.102 0.4267 5.3625
1.171 2.4 5.4 2 4 1 82.264 41.132 0.4270 5.3657
1.170 1.3 2.9 2 2 5 82.315 41.158 0.4272 5.3684
1.170 1.3 2.9 0 4 3 82.315 41.158 0.4272 5.3684
1.143 0.4 0.9 4 1 3 84.654 42.327 0.4371 5.4926
1.131 5.8 13.6 4 2 2 85.850 42.925 0.4421 5.5553
1.130 6.0 14.0 2 4 2 85.913 42.956 0.4423 5.5585
1.129 2.4 5.6 2 0 6 85.964 42.982 0.4425 5.5612
1.129 5.8 13.6 0 2 6 86.001 43.000 0.4427 5.5631
1.117 1.7 4.0 3 3 3 87.114 43.557 0.4473 5.6208
1.117 1.2 2.8 1 3 5 87.182 43.591 0.4476 5.6243
1.082 5.0 12.2 4 0 4 90.715 45.357 0.4618 5.8037
1.081 5.0 12.2 0 4 4 90.797 45.399 0.4622 5.8079
1.071 0.6 1.5 4 2 3 91.914 45.957 0.4666 5.8634
1.071 1.7 4.2 2 4 3 91.973 45.986 0.4668 5.8663
1.040 1.9 4.8 5 1 0 95.476 47.738 0.4804 6.0368
1.039 4.8 12.2 3 3 4 95.592 47.796 0.4808 6.0424
1.039 4.8 12.2 1 5 0 95.592 47.796 0.4808 6.0424
1.039 4.6 11.7 2 2 6 95.661 47.830 0.4811 6.0457
1.030 2.5 6.4 1 5 1 96.813 48.407 0.4855 6.1004
1.002 6.8 17.9 5 1 2 100.357 50.179 0.4985 6.2650
1.002 8.3 21.9 4 2 4 100.434 50.217 0.4988 6.2685
1.001 18.1 47.8 2 4 4 100.503 50.251 0.4991 6.2716
1.001 18.1 47.8 1 5 2 100.503 50.251 0.4991 6.2716
1.001 6.9 18.2 1 3 6 100.552 50.276 0.4993 6.2738
1.001 6.9 18.2 3 1 6 100.552 50.276 0.4993 6.2738
0.992 1.0 2.7 0 4 5 101.776 50.888 0.5037 6.3291
0.976 0.3 0.8 4 3 3 104.137 52.068 0.5120 6.4338
0.976 0.3 0.8 1 4 5 104.223 52.111 0.5123 6.4376
0.960 0.3 0.8 5 1 3 106.606 53.303 0.5205 6.5404
0.960 2.7 7.4 3 3 5 106.718 53.359 0.5208 6.5451
0.960 2.7 7.4 1 5 3 106.718 53.359 0.5208 6.5451
0.937 3.1 8.7 4 4 0 110.434 55.217 0.5331 6.6995
0.936 1.7 4.8 0 0 8 110.666 55.333 0.5339 6.7089
0.930 1.3 3.7 4 4 1 111.729 55.865 0.5373 6.7517
0.929 1.3 3.7 2 4 5 111.850 55.925 0.5377 6.7565
0.909 7.0 20.4 3 5 0 115.680 57.840 0.5495 6.9054
0.909 7.0 20.4 5 1 4 115.680 57.840 0.5495 6.9054
0.909 4.2 12.2 1 5 4 115.798 57.899 0.5499 6.9099
0.909 4.2 12.2 4 0 6 115.798 57.899 0.5499 6.9099
0.908 3.4 9.9 0 4 6 115.901 57.950 0.5502 6.9138
0.908 3.4 9.9 1 1 8 115.901 57.950 0.5502 6.9138
0.903 0.8 2.3 5 3 1 116.976 58.488 0.5534 6.9541
0.903 1.8 5.3 3 5 1 117.080 58.540 0.5537 6.9580
0.902 0.6 1.8 1 3 7 117.252 58.626 0.5542 6.9644
0.884 5.1 15.3 5 3 2 121.119 60.559 0.5653 7.1037
0.884 5.1 15.3 6 0 0 121.119 60.559 0.5653 7.1037
0.884 5.2 15.6 3 5 2 121.220 60.610 0.5656 7.1072
0.884 5.2 15.6 0 6 0 121.220 60.610 0.5656 7.1072
0.883 7.8 23.4 3 3 6 121.319 60.659 0.5658 7.1107
0.883 4.5 13.5 0 2 8 121.434 60.717 0.5662 7.1147
0.883 4.5 13.5 2 0 8 121.434 60.717 0.5662 7.1147
0.878 0.7 2.1 4 4 3 122.609 61.304 0.5694 7.1552
0.877 1.3 3.9 0 6 1 122.692 61.346 0.5696 7.1580